Chemical Formula: C10H18Cl2N2O8Pt
Molecular Weight: 560.2440
m/z: 559.0088 (100.0%), 558.0067 (97.4%), 560.0090 (74.6%), 561.0058 (63.9%), 560.0037 (62.3%), 562.0060 (47.7%), 562.0119 (21.2%), 564.0089 (13.5%), 560.0121 (10.8%), 559.0100 (10.5%), 563.0029 (10.2%), 562.0008 (10.0%), 561.0123 (8.1%), 564.0031 (7.6%), 562.0092 (6.9%), 561.0071 (6.7%), 563.0094 (5.2%), 556.0051 (2.3%), 563.0153 (2.3%), 566.0060 (2.2%), 561.0130 (1.6%), 560.0109 (1.6%), 558.0021 (1.5%), 565.0123 (1.5%), 562.0132 (1.2%), 564.0062 (1.1%), 563.0041 (1.1%), 563.0101 (1.1%), 562.0080 (1.0%)
Elemental Analysis: C, 21.44; H, 3.24; Cl, 12.66; N, 5.00; O, 22.85; Pt, 34.82
参考路线：
Compound 1: CAS 14096-51-6, Dichloro(ethylenediamine)platinum(II), commercially available
Compound 2: CAS 54361-80-7
Compound 3: CAS 929602-93-7
Proposed synthesis method:
Step 1:
- Suspend ~ 1 g of Compound 1 in 22 mL of triply distilled water.
- Add an amount of 11 mL of 30% H2O2 to the mixture.
- Stir the mixture for 3 hours at 30 °C (in the dark).
- Reduce the volume of the clear yellow solution obtained on a rotavapor and cool in the fridge.
- Precipitate the mixture with a sufficient amount of cold acetone. Finalize the precipitation with the help of ultrasonic waves.
- Filter the final product.
- Wash the mixture with acetone and dry in vacuo.
- Use column chromatography purification to obtain Compound 2 and dry the product in vacuo.
Step 2:
- Suspend succinic anhydride and Compound 2 in dry DMF (molar ratio: ~ 5:1).
- Stir the reaction mixture at 60 °C for 8 hours.
- Remove DMF under reduced pressure.
- Suspend the residue in acetone with the help of ultrasonic waves.
- Filter the reaction mixture.
- Wash the mixture with acetone and dry in vacuo.
- Use column chromatography purification to obtain Compound 3 and dry the product in vacuo.
需要数据：
- Yield
- Elemental analysis
- Mass spectrum
- 1H NMR
- 13C NMR
- 15N NMR
- 195Pt NMR
- 1H−1H COSY (optional)
- 1H−13C HSQC (optional)
- 1H−15N HSQC (optional)
- 1H−13C HMBC (optional)
- IR spectrum (optional)
