实验工艺可参考如下文献：

1 Crystalline Graphdiyne Nanosheets Produced at a Gas/Liquid or Liquid/Liquid Interface. Ryota Matsuoka, Ryota Sakamoto,,§ Ken Hoshiko, Sono Sasaki, Hiroyasu Masunaga,Kosuke Nagashio,and Hiroshi Nishihara. Journal of the American Chemical Society

2  Ultrathin Graphdiyne Nanosheets in-situ Grown on Copper Nanowires and its Performance as Lithium-Ion Battery Anodes. Hong Shang, Zicheng Zuo , Liang Li, Fan Wang, Huibiao Liu, Yongjun Li , and Yuliang Li. Angewandte Chemie

3 Synthesis of Graphdiyne Nanowalls Using Acetylenic Coupling Reaction. Jingyuan Zhou,Xin Gao, Rong Liu, Ziqian Xie,Jin Yang, Shuqing Zhang,Gengmin Zhang,Huibiao Liu,Yuliang Li,Jin Zhang, and Zhongfan Liu.   Journal of the American Chemical Society